Bruker Avance III HD 400 MHz spectrometer with a BBFO 31P-15N probe and a TXI 1H / 13C / 31P three-channel probe

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Description

NMR spectrometer works in a continuous mode 24 hours a day / 7 days a week. 1D NMR spectra are routinely performed: 1H, 31P, 13C, 19F, 11B, 29Si, 77Se, and 2D NMR heterocorrelation spectra: COSY, ROESY, HMBC, HMQC as well as variable temperature measurements both at low and elevated temperature. The spectra made allow to determine the structure of new chemical compounds in a solution as well as to confirm the structure or purity of known compounds. NMR spectroscopy allows to monitor the course of reactions and determine their mechanisms, it also allows to monitor the course of technological processes.

Examples of research articles:
Publications

10.1021/acs.inorgchem.0c03563; 10.1021/acs.inorgchem.7b01374; 10.1039/C9CC00621D

Details

Type of infrastructure:
'Core Lab' laboratory
Strategic infrastructure:
No
Accessibility
scientific research
commercial activities

Manager / operator

Manager

Manager's name
dr hab. inż. Rafał Grubba
Manager's e-mail
rafal.grubba@pg.edu.pl

Manufacturer

Manufacturer
Bruker
Year of production
2015

Laboratory where the equipment is located

Name of the laboratory
Laboratory of Nuclear Magnetic Resonance

Location

University
Gdańsk University of Technology

Access rules

Access rules

The rules of using the equipment will be consistent with the research infrastructure management system being developed. The elements of this system include the method of reporting the demand for the performance of tests, the appointment of a person responsible for the performance of the tests, and the rules governing the intellectual property of the results. An element of the system will also be the settlement for the performed tests, allowing for free testing (in the case of joint publication or on the basis of reciprocity using the apparatus).